Wednesday, May 11, 2016

Practical 2: Deodorants and Antiperspirants




Name of experiment: Deodorants and Antiperspirants
Date of experiment: 27th April 2016
Lecturer: Prof. Madya Dr. Ng Shiow Fern 
Group members: 
1. Alicia Ong Su May (A152332)
2. Tasneem binti Mahayudin (A152348)
3. Mohamad Azmi bin Isahak (A153317)
4. Nor Afiqah Bt Mohd Nasir Tan (A154096)
5. Abdul Hafiz bin Zakaria (A144377)

INTRODUCTION
            Deodorants are classified and regulated as cosmetics by the U.S. Food and Drug Administration (FDA) and are designed to eliminate odour. Deodorants are often alcohol-based. Alcohol initially stimulates sweating, but may also temporarily kill bacteria. Other active ingredients in deodorants include sodium stearate, sodium chloride and stearyl alcohol. Deodorants can be formulated with other, more persistent antimicrobials such as triclosan that slows down bacterial growth or with metal chelating agents such as EDTA. Deodorants may contain perfume fragrances or natural essential oils intended to mask the odour of perspiration.
            Deodorants and antiperspirants are preparations that can mask, remove or reduce the unpleasant odour on the body due to sweat. Sweat on its own does not generally have a smell, bacteria present on the surface of the skin digests the sweat and the digestion and breakdown products cause the odour. Therefore, a deodorant functions by decreasing the bacteria population on the skin or by adding fragrance to the body to overcome foul odour. On the other hand, an antiperspirant functions by reducing the production of sweat through its astringent property.
            Antiperspirants are typically applied to the underarms, while deodorants may also be used on feet and other areas in the form of body sprays (aerosol), sticks, creams and roll ons.

OBJECTIVE
1.      To differentiate the functions of each of the different ingredients used in the making of product
2.      To understand the function and rationale of differentiating the amount or type of fragrance incorporated in the product
3.      To evaluate the quality of the finished product

APPARATUS
1.        Evaporating dish
2.        Water bath
3.        Electronic balance
4.        Weighing boat
5.        Glass rod
6.        Thermometer
7.        Measuring cylinder

MATERIALS
1.        Beeswax
2.        Cocoa butter
3.        Coconut oil
4.        Silicone oil
5.        Vitamin E oil
6.        Corn starch
7.        Different types of essential oil/perfumes

METHOD AND PROCEDURE
1.      The beeswax and the cocoa butter are heated until they have just melted. Then, the coconut, silicone, and vitamin E oils are added.
2.      When all the oils and fats have melted, the essential oils/perfumes are added.
3.      Using a hand mixer, the corn starch is mixed in until homogenous.
4.      The molten mixture is poured into the container and allowed to cool until it hardens.

RESULTS
Formulation 1: Citrus
Ingredients
Percentage (%)
Weight
Beeswax
20
4.0
Cocoa butter
30
6.0
Coconut oil
30
6.0
Silicone oil
3
0.6
Vitamin E oil
2
0.4
Corn starch
12
2.4
Perfume (Citrus)
<3
0.4


Formulation 2: Topaz
Ingredients
Percentage (%)
Weight
Beeswax
20
4.0
Cocoa butter
30
6.0
Coconut oil
30
6.0
Silicone oil
3
0.6
Vitamin E oil
2
0.4
Corn starch
12
2.4
Perfume (Topaz)
<3
0.4

Formulation 3: Rose
Ingredients
Percentage (%)
Weight
Beeswax
20
4.0
Cocoa butter
30
6.0
Coconut oil
30
6.0
Silicone oil
3
0.6
Vitamin E oil
2
0.4
Corn starch
12
2.4
Perfume (Rose)
<3
0.4

Formulation 4: Flora
Ingredients
Percentage (%)
Weight
Beeswax
20
4.0
Cocoa butter
30
6.0
Coconut oil
30
6.0
Silicone oil
3
0.6
Vitamin E oil
2
0.4
Corn starch
12
2.4
Perfume (Flora)
<3
0.4


Formulation 5: Apple
Ingredients
Percentage (%)
Weight
Beeswax
20
4.0
Cocoa butter
30
6.0
Coconut oil
30
6.0
Silicone oil
3
0.6
Vitamin E oil
2
0.4
Corn starch
12
2.4
Perfume (Apple)
<3
0.4

EVALUATION AND STABILITY TESTING RESULTS

All of the deodorant products were tested by the group members. A simple questionnaire was designed to evaluate the effectiveness of each product and whether the fragrance incorporated is irritating to the skin. The following are the results from the questionnaire:

Aspect
Strongly disagree
Disagree
Not sure
Agree
Strongly agree
I like the smell of the deodorant.


1
3
1
The fragrance effectively masked my body odour.

1
2
2

The fragrance could last throughout the whole day (9 hours).
1
2
1
1

The fragrance vanished after my daily activities.


1
3
1
I feel comfortable wearing the deodorant.


1
3
1
The deodorant caused irritation to my underarm.
3
2




The stability of the products was evaluated by placing in warm position (room temperature) and also in sunny position. The results of the evaluation:

In warm position (room temperature):
Product
Observation
Citrus
No changes in smell, colour and texture
Topaz
No changes in smell, colour and texture
Rose
No changes in smell, colour and texture
Flora
No changes in smell, colour and texture
Apple
No changes in smell, colour and texture

At room temperature


In sunny position:
Product
Observation
Citrus
No changes in smell and colour but sweating occurred
Topaz
No changes in smell and colour but sweating occurred
Rose
No changes in smell and colour but sweating occurred
Flora
No changes in smell and colour but sweating occurred
Apple
No changes in smell and colour but sweating occurred

Under the hot sun
Citrus

Topaz

Rose

Flora

Apple



DISCUSSION
Deodorant and antiperspirant are different products. Antiperspirant controls sweat and body odour in two ways which are by preventing sweat reaching the skin surface and by reducing the bacteria that causes body odour via antimicrobial ingredients. Deodorants differ from antiperspirants as they only contain antimicrobial agents to prevent body odour. They do not control the flow of sweat. Both antiperspirants and deodorants often contain fragrances to help mask the smell of body odour.
In this experiment we have prepared five different formulations of deodorant which contains different types of perfumes. All the formulations contain the same amount of ingredients. The ingredients for the formulation of deodorant are 4 g of beeswax, 6 g of coca butter, 6 g of coconut oil, 0.6 g of silicone oil, 0.4 g of vitamin E oil, 2.4 g of corn starch and 0.4 g of perfume. Each product contains citrus, topaz, rose, flora and apple odour respectively. Precaution when using essential oil/perfumes has to be taken as they may cause instability to the products and irritation to the skin.
Each of the group members is required to test the deodorants. A simple questionnaire was devised that allow each person to compare the effectiveness of each product and whether the fragrance incorporated is irritating to the skin. Each consumer must put the deodorant on the underarm and after exactly 9 hours of normal daily activities, and the consumer must fill in the questionnaire.
Based on the results obtained, most of the consumers like the smell of the deodorant. Secondly, there were two people who agree and only one person who disagree that the fragrance effectively masked their body odour. Two people were not sure whether the fragrance masked their body odour. For the third question, two people disagree while each of the three people strongly disagree, not sure and agree respectively that the fragrance could last throughout the whole day (9 hours). Next, most of the consumers agree and only two people were not sure and strongly agree respectively that the fragrance vanished after their daily activities. The same goes to the next question whether they felt comfortable or not when wearing the deodorant. Lastly, all disagree (strongly disagree and disagree combined) that the deodorant caused irritation to their underarm.
For the stability test, all the deodorants are placed in one warm (room temperature) and sunny position. It was found that all the products did not have changes in smell, colour and texture when placed in warm position which is at room temperature. While in the sunny position, all the deodorants also did not have any changes in smell and colour but sweating was occurred. This test is important so that consumers are aware that the storage condition will affect the quality of deodorant.

CONCLUSION

As a conclusion, deodorants and antiperspirants are preparations that can mask, remove or reduce the unpleasant odour on the body due to sweat. Through the practical, we were able to differentiate the different functions of each ingredient in the formula and evaluate the quality of our products. Thus, we can improve our formulation for better quality, appearances and function of the products in the future. Different people have different preferences of fragrance, so we need to prepare a variety of fragrances to meet their demands. In this experiment, we only prepared five different fragrances which are citrus, topaz, rose, flora and apple. We have tested the effectiveness by using the deodorants and answering the questionnaire. Besides, we have also tested the stability of the deodorants by observing the changes when placed at room temperature and under the hot sun. It can be concluded that the storage conditions affect the stability of the deodorants. Hence, deodorants should be kept at room temperature and not be exposed to high heat and temperature. 

REFERENCES